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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 413979Generated: October 31, 2026

Acrolein → 6,6-dimethylhept-1-en-4-yn-3-ol

https://huagongshe.com/reaction/413979

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcroleinHCID 7847—
Reactant3,3-Dimethyl-1-butyneHCID 13512—
ReactantButyllithiumHCID 178418339—
Product6,6-dimethylhept-1-en-4-yn-3-olHCID 10975561—

Reaction Conditions

Temperature-75 °C

Reaction Steps

Reacting t-butylacetylene at −20° C. with butyllithium, cooling the reaction mixture to −75° C. and reacting it with acrolein to give 6,6-dimethylhept-1-en-4-yn-3-ol.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06570044B2
Source datasetuspto-grants-2003_05
ORD IDord-5567b88f6f28441c8585afa6254808db
Source noteuspto-grants-2003_05