Isopropanol → HCID 14390621, compound

Participants

Reaction Steps

A mixture prepared from 1-(4-amino-2-methyl-3-quinolinyl)-propanone (8 g), sodium borohydride (3 g), 75 ml of isopropanol and 25 ml of methanol was stirred twenty hours at ambient temperature. The reaction mixture was concentrated and stirred with water, and the product which separated was collected and dried to 8 g of solid, mp 220°-230°. This material was recrystallized from absolute ethanol to give 4.6 g of crystals, mp 240°-241°.

Provenance & Evidence