Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Methyl 2-pentenoate | HCID 5364718 | — |
| Product | Methyl 3-piperidinovalerate | HCID 14178339 | — |
Reaction Steps
A mixture of 500 g of methyl 2-trans-pentenoate and 372 g of piperidine was heated at 65° C. for 17 hours and then at 100° C. for 24 hours. After distillation over a Vigreux column, 562 g (64% of theory) of methyl 3 -piperidinovalerate of boiling point 64° C./2 mbar, nD20 =1.4592, were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04791220 |
|---|
| Source dataset | uspto-grants-1988_12 |
|---|
| ORD ID | ord-8dd5369b1df347b7a55961ccede03f61 |
|---|
| Source note | uspto-grants-1988_12 |
|---|
