Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Methyl 2-pentenoate | HCID 5364718 | — |
| Product | Methyl 3-morpholinovalerate | HCID 20035200 | — |
Reaction Steps
A mixture of 171 g of methyl 2-trans-pentenoate and 130.5 g of morpholine was heated for 46 hours at 100° C. After distillation of the reaction mixture over a Vigreux column, 179 g (59% of theory) of methyl 3-morpholinovalerate of boiling point 85° C./0.4 mbar, nD20 =1.4610, were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04791220 |
|---|
| Source dataset | uspto-grants-1988_12 |
|---|
| ORD ID | ord-6e72a1f644624095b6631187d859dcda |
|---|
| Source note | uspto-grants-1988_12 |
|---|
