Triethylamine → HCID 53837822, compound

Participants

Reaction Steps

A mixture of 4'-[(6-hydroxyhexyl)methylamino]-4-methylsulfonylstilbene (5.00 g, 12.9 mmol) was treated with triethylamine (1.63 g, 16.2 mmol) and acryloyl chloride (1.46 g, 16.2 mmol) as above. The product was purified by chromatography on silica gel (CH2CL2 eluent) and recrystallization from acetone/hexanes to yield 2.10 g (37%) of a yellow solid, mp 88°-90° C.

Provenance & Evidence