HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → 2-(Aminomethyl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | 4-tert-Butylphenol | HCID 7393 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | 2-(Aminomethyl)phenol | HCID 70267 | — |
Reaction Steps
An o-hydroxybenzylamine compound of the present invention composition was prepared according to the procedure of Example 1, except that 50 g of 4-t-butylphenol was employed in place of the Bisphenol-A, 20.1 g of ethanolamine was employed in place of the 2-(methylamino)ethanol, and that heating of the reactants was only begun after the formaldehyde addition was completed. A 0.5 g sample of the product was dissolved in 500 ml of ethanol/water (1:4 by volume) and the pH of the solution was adjusted to 3.0 with phosphoric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792355 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-7486f9fc336349f2b2dc1e0a870090b4 |
| Source note | uspto-grants-1988_12 |