HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 2-[(4-Ethylphenyl)methyl]benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 2-(4-Ethylbenzoyl)benzoic acid | HCID 70852 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-[(4-Ethylphenyl)methyl]benzoic acid | HCID 17858694 | — |
Reaction Steps
(b.1) A solution of 2-(4-ethylbenzoyl)benzoic acid in acetic acid (115 ml) and the dimethylformamide (115 ml) containing 10% palladium on carbon (4.9 g) was shaken in a hydrogen atmosphere at 60 p.s.i. for 6 hours. The solution was then filtered and the filtrate was added to water (2000 ml), producing a precipitate of 2-(4-ethylbenzyl)benzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792551 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-4b61096b07e249d9908254f334bdf05e |
| Source note | uspto-grants-1988_12 |