Sulfuric Acid → HCID 21280798, compound

HRID 414481Notes

Reaction equation

HRID 414481 reaction equation
C(O)(=O)C.[CH:5]1[C:18]2[C:9](=[CH:10][C:11]3[C:16]([C:17]=2[O:19][CH2:20][CH2:21][CH2:22][NH2:23])=[CH:15][CH:14]=[CH:13][CH:12]=3)[CH:8]=[CH:7][CH:6]=1.[S:24](=[O:28])(=[O:27])([OH:26])[OH:25]>O>[S:24](=[O:26])(=[O:25])([OH:28])[OH:27].[CH:15]1[C:16]2[C:11](=[CH:10][C:9]3[C:18]([C:17]=2[O:19][CH2:20][CH2:21][CH2:22][NH2:23])=[CH:5][CH:6]=[CH:7][CH:8]=3)[CH:12]=[CH:13][CH:14]=1

Participants

4

Reactant 2

HCID 1118Sulfuric AcidHCID 86122433HCID 86122433, compound

Product 1

HCID 21280798HCID 21280798, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

1-(9-anthryloxy)-3-aminopropane acetate (1.0 g) is dissolved in 50 ml water containing a stoichiometric equivalent to sulfuric acid, and the solution evaporated to dryness. The product is suspended in ethanol and filtered, air dried and recrystallized from methanol/acetone to yield 1-(9-anthryloxy)-3-aminopropane bisulfate.

Workup

  1. customthe solution evaporated to dryness
  2. filtrationfiltered
  3. customair dried
  4. customrecrystallized from methanol/acetone

Sources & evidence

ORD record
ord-9edbae6350bc4a65a42545d81b0c75bb
Source dataset
uspto-grants-1988_12
Patent number
US04792551

Reaction notes

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