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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 414553Generated: November 1, 2026

Benzoyl chloride → 120067-47-2

https://huagongshe.com/reaction/414553

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzoyl chlorideHCID 7412—
ReactantHydrocarbostyrilHCID 64796—
ReactantAluminum(III) ChlorideHCID 6451240—
SolventCarbon DisulfideHCID 6348—
Product120067-47-2HCID 14373255—

Reaction Steps

A mixture of 2.2 g of 3,4-dihydrocarbostyril, 3.21 g of benzoyl chloride and 13 g of aluminum chloride in 50 ml of carbon disulfide was refluxed for 2 days. The reaction mixture was poured onto ice water and the resulting solid filtered off, washed with water and dried under reduced pressure to yield 6-benzoyl-3,4-dihydrocarbostyril, m.p. 205°-207° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04792561
Source datasetuspto-grants-1988_12
ORD IDord-0127fe44c23c46e0b4d89c8475022a79
Source noteuspto-grants-1988_12