HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → 120067-47-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Hydrocarbostyril | HCID 64796 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Carbon Disulfide | HCID 6348 | — |
| Product | 120067-47-2 | HCID 14373255 | — |
Reaction Steps
A mixture of 2.2 g of 3,4-dihydrocarbostyril, 3.21 g of benzoyl chloride and 13 g of aluminum chloride in 50 ml of carbon disulfide was refluxed for 2 days. The reaction mixture was poured onto ice water and the resulting solid filtered off, washed with water and dried under reduced pressure to yield 6-benzoyl-3,4-dihydrocarbostyril, m.p. 205°-207° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792561 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-0127fe44c23c46e0b4d89c8475022a79 |
| Source note | uspto-grants-1988_12 |