Propanoyl bromide, 2-bromo- → HCID 21281525, compound

HRID 414660Notes

Reaction equation

HRID 414660 reaction equation
[OH:1][CH2:2][CH2:3][N:4]([CH3:9])[C:5](=[O:8])[O:6][CH3:7].[Br:10][CH:11]([CH3:15])[C:12](Br)=[O:13]>>[Br:10][CH:11]([CH3:15])[C:12]([O:1][CH2:2][CH2:3][N:4]([CH3:9])[C:5](=[O:8])[O:6][CH3:7])=[O:13]

Participants

3

Reactant 2

HCID 79047Propanoyl bromide, 2-bromo-HCID 568300Carbamic acid, (2-hydroxyethyl)methyl-, methyl ester

Product 1

HCID 21281525HCID 21281525, compound

Procedure

by using methyl N-(2-hydroxyethyl)-N-methyl-carbamate and 2-bromopropionyl bromide there is obtained methyl N-[2-(2-bromopropionyloxy)-ethyl]-N-methyl-carbamate, 1H-NMR (CDCl3, 60 MHz) 4.35 ppm (q, 1H), 4.32 ppm (t, 2H), 3.75 ppm (s, 3H), 3.58 ppm (t, 2H), 3.0 ppm (s, 3H), 1.82 ppm (d, 3H);

Sources & evidence

ORD record
ord-c28b9494e8f943a48ebb5ccdc46bb5aa
Source dataset
uspto-grants-1988_12
Patent number
US04792616

Reaction notes

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