HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 4-Methyl-6-nitro-7-hydroxy-1-indanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 7-Hydroxy-4-methyl-1-indanone | HCID 12436244 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 4-Methyl-6-nitro-7-hydroxy-1-indanone | HCID 13604142 | — |
Reaction Steps
Into a solution of 25.6 g of 4-methyl-7-hydroxy-1-indanone in 250 ml of acetic acid was added 19.4 ml of acetic anhydride and a solution of 15.4 ml of concentrated nitric acid in 50 ml of acetic acid gradually. The reaction mixture was concentrated to drynsss, and the residue was washed with ether to obtain 25.7 g of 4-methyl-6-nitro-7-hydroxy-1-indanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04792628 |
| Source dataset | uspto-grants-1988_12 |
| ORD ID | ord-5cb9e452ae114983b72b93924d0f9940 |
| Source note | uspto-grants-1988_12 |