化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → 4-Methyl-6-aminomethyl-7-hydroxy-1-indanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 4-Methyl-6-alpha-chloroacetylaminomethyl-7-hydroxy-1-indanone | HCID 13604141 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 4-Methyl-6-aminomethyl-7-hydroxy-1-indanone | HCID 13604144 | — |
反応手順
3 Grams of 4-methyl-6-α-chloroacetylaminomethyl-7-hydroxy-1-indanone and a solution of 30 ml of concentrated sulfuric acid in 60 ml of ethanol were refluxed by heating for 8 hours. The solvent was removed by evaporation, the residue thus obtained was recrystallized from ethanol to obtain 1 g of 4-methyl-6-aminomethyl-7-hydroxy-1-indanone.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04792628 |
| 出典データセット | uspto-grants-1988_12 |
| ORD ID | ord-d178894b4e4c4482b7509e98b99d4b09 |
| 出典メモ | uspto-grants-1988_12 |