Hydrazine → HCID 14098875, compound

HRID 414711Notes

Reaction equation

HRID 414711 reaction equation
[C:1]([N:4]1[CH2:9][CH2:8][N:7]2[CH:10]=[C:11]([C:13]([O:15]CC)=O)[N:12]=[C:6]2[CH2:5]1)(=[O:3])[CH3:2].[NH2:18][NH2:19]>>[C:1]([N:4]1[CH2:9][CH2:8][N:7]2[CH:10]=[C:11]([C:13]([NH:18][NH2:19])=[O:15])[N:12]=[C:6]2[CH2:5]1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 9321HydrazineHCID 21280349HCID 21280349, compound

Product 1

HCID 14098875HCID 14098875, compound

Procedure

6 g of the ester thereby obtained, in 10 ml of hydrazine, are brought to the refluxing temperature for 20 min. The excess hydrazine is evaporated off and the oil obtained purified by chromatography on a silica column (methylene chloride/methanol/ammonia solution 19:10:1).

Workup

  1. customThe excess hydrazine is evaporated off
  2. customthe oil obtained
  3. custompurified by chromatography on a silica column (methylene chloride/methanol/ammonia solution 19:10:1)

Sources & evidence

ORD record
ord-345ddb17d64f466dabc0bbb768e7e74c
Source dataset
uspto-grants-1988_12
Patent number
US04794120

Reaction notes

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