Carbon Dioxide → HCID 178527662, compound

HRID 414882Notes

Reaction equation

HRID 414882 reaction equation
C(=O)([O-])[O-].[Ag+2:5].[CH2:6]([S:11]([OH:14])(=[O:13])=[O:12])[S:7]([OH:10])(=[O:9])=[O:8].C(=O)=O>O>[CH2:6]([S:11]([O-:14])(=[O:13])=[O:12])[S:7]([O-:10])(=[O:9])=[O:8].[Ag+2:5]

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 10427Methanedisulfonic acidHCID 178418647HCID 178418647, compound2×

Product 1

HCID 178527662HCID 178527662, compoundYield 123.7%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Silver carbonate (20 g, 0.0725 moles) was added to methanedisulfonic acid (25.55 g 50% solution in water) and diluted in 25 mL of distilled water while stirring. The silver carbonate dissolved with effervescence of carbon dioxide. After the reaction was complete, any remaining insoluble material was removed by filtration and the filtrate was stripped of water was removed under vacuum to give 25.3 g of pure silver methanedisulfonate.

Workup

  1. customany remaining insoluble material was removed by filtration
  2. customwas removed under vacuum

Sources & evidence

ORD record
ord-7e11e4253b7d44f2a2c4ac9c3e72ef63
Source dataset
uspto-grants-2012_01
Patent number
US08088548B2

Reaction notes

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