HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 135995084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 58407891 | HCID 58407891 | — |
| Product | HCID 135995084 | HCID 135995084 | — |
Reaction Steps
In analogy to the preparation of Example 1, 100 mg (0.31 mmol) of 4-(methylsulphanyl)-6-oxo-2-[3-(trifluoromethyl)benzyl]-1,6-dihydropyrimidine-5-carbonitrile are reacted with 262 mg (3.07 mmol) of piperidine to give 26 mg (22% of theory) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088769B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-4d5cd944bf294ca18178ce5ddc8a6cf8 |
| Source note | uspto-grants-2012_01 |