Ammonia → HCID 46847386, compound

Participants

Reaction Steps

Methyl 2-(4-(pyridin-3-yl)phenyl)benzo[d]oxazole-7-carboxylate (600 mg, 1.81 mmol) was added to ammonia in methanol (30 ml) and the mixture was stirred at room temperature for 3 days. Then the solid was filtered, washed with methanol, dried in vacuum. 550 mg 2-(4-(pyridin-3-yl)phenyl)benzo[d]oxazole-7-carboxamide was obtained, yield: 96%. LC-MS (ESI) m/z: 316 (M+1)+.

Provenance & Evidence