Acetonitrile → HCID 59402730, compound

HRID 415575Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9]([NH2:11])=[O:10].[CH3:12][C:13]#N>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:9][CH2:3][CH2:2][CH2:7][CH2:6][CH2:5][CH2:4][CH2:13][CH3:12])=[CH:4][C:3]=1[C:9]([NH2:11])=[O:10]

Participants

Reactant 2

HCID 6342Acetonitrile

HCID 57422942HCID 57422942, compound

Product 1

HCID 59402730HCID 59402730, compoundYield 80%

Procedure

Synthesised from 2-chloro-5-hydroxybenzenecarboxamide according to Method B, scheme 2. Yield 80%, HPLC-MS (method 1): m/z 339 [M+H+CH3CN]+, Rt=5.29 min.

Sources & evidence

ORD record: ord-608e6a52076141f9bab6a5a0c8f1e563
Source dataset: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08088791B2

Reaction notes

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