HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → 6-Chloro-2-fluoro-3-methoxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 6-Chloro-2-fluoro-3-methoxybenzoic acid | HCID 3856039 | — |
| Product | 6-Chloro-2-fluoro-3-methoxybenzamide | HCID 17999360 | 85% |
Reaction Steps
Synthesised from commercially available 6-chloro-2-fluoro-3-methoxybenzenecarboxylic acid according to Method A, scheme 1. Yield 85%, mp 154-156° C., HPLC-MS (method 1): m/z 245 [M+H+CH3CN]+, Rt=2.37 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088791B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-08d1a11d2190433f8041b03d146c33d7 |
| Source note | uspto-grants-2012_01 |