HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloro-2-benzothiazolamine → 3-[(6-Chloro-1,3-benzothiazol-2-yl)methoxy]-2,6-difluorobenzenecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloro-2-benzothiazolamine | HCID 7226 | — |
| Reactant | 3-(Cyanomethoxy)-2,6-difluorobenzenecarboxamide | HCID 59402804 | — |
| Product | 3-[(6-Chloro-1,3-benzothiazol-2-yl)methoxy]-2,6-difluorobenzenecarboxamide | HCID 46237139 | 38% |
Reaction Steps
Synthesised from 6-chloro-1,3-benzothiazol-2-amine and 3-(cyanomethoxy)-2,6-difluorobenzene carboxamide, according to Method K, scheme 26. Yield 38% (second step), mp 190-191° C., HPLC-MS (method 1): m/z 355 [M+H]+, Rt=3.85 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088791B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-b46349a9f1e640b98d4e7cf12a1b7d27 |
| Source note | uspto-grants-2012_01 |