HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroquinoxaline → 2-(3-Iodobenzyl)-9-(quinoxalin-2-yl)-2,9-diazaspiro[5.5]undecan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroquinoxaline | HCID 238938 | — |
| Reactant | 3-Iodobenzyl bromide | HCID 2759361 | — |
| Reactant | 2,9-Diazaspiro[5.5]undecan-1-one | HCID 17750924 | — |
| Product | 2-(3-Iodobenzyl)-9-(quinoxalin-2-yl)-2,9-diazaspiro[5.5]undecan-1-one | HCID 67252042 | — |
Reaction Steps
The title compound was synthesized in analogy to method A from 2,9-diazaspiro[5.5]undecan-1-one (TFA salt) [1190586-22-1], 3-iodobenzyl bromide [49617-83-6] and 2-chloroquinoxaline [1448-87-9]. [LCMS RtF=1.99 min, [M+H]+=513.0].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08530648B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-4e5150db0c1b4210a85f3e441aaf8ac5 |
| Source note | uspto-grants-2013_09 |