HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-4-hydroxybenzaldehyde → 3-(3-Bromo-4-hydroxyphenyl)-1-(5-(4-(trifluoromethyl)phenyl)thien-2-yl)prop-2-en-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-4-hydroxybenzaldehyde | HCID 76308 | — |
| Reactant | 1-(5-(4-(Trifluoromethyl)phenyl)thiophen-2-yl)ethan-1-one | HCID 4191494 | — |
| Product | 3-(3-Bromo-4-hydroxyphenyl)-1-(5-(4-(trifluoromethyl)phenyl)thien-2-yl)prop-2-en-1-one | HCID 66623825 | — |
Reaction Steps
3-(3-Bromo-4-hydroxyphenyl)-1-(5-(4-(trifluoromethyl)phenyl)thien-2-yl)prop-2-en-1-one is prepared from 1-(5-(4-(trifluoromethyl)phenyl)thien-2-yl)ethanone and 3-bromo-4-hydroxybenzaldehyde according to general procedure B. The evaporation residue is crystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088819B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-314c311cf9f74989989d50501c1c748a |
| Source note | uspto-grants-2012_01 |