反应详情

2-Iodo-3-hydroxy-6-methylpyridine (835 mg) and iodomethane (3 mL) were added in glass sealed cube, and the reaction mixture was reacted at 130° C. for 4 h and at 180° C. for 1 h. The reaction mixture was completely evaporated to give 3-hydroxy-2-iodo-1,6-dimethylpyridinium iodide (2-014-02) (1.42 g).

1. customsealed cube
2. customthe reaction mixture was reacted at 130° C. for 4 h and at 180° C. for 1 h
3. customThe reaction mixture was completely evaporated