HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 46928887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 59496849 | HCID 59496849 | — |
| Product | HCID 46928887 | HCID 46928887 | 79.1% |
Reaction Steps
A similar procedure as described in Example 43, step 5 was used, starting from 4-[2-(2-ethoxycarbonyl-ethyl)-3-{6-[3-ethoxy-5-(1H-indol-6-yl)-phenoxy]-hexyl}-phenoxy]-butyric acid ethyl ester (111 mg, 0.17 mmol) and 1.0 N aqueous sodium hydroxide (1.7 mL) to afford 4-[2-(2-carboxy-ethyl)-3-{6-[3-ethoxy-5-(1H-indol-6-yl)-phenoxy]-hexyl}-phenoxy]-butyric acid (79 mg, 78%) as a light brown solid: ES(+)-HRMS m/e calcd for C35H41NO7 (M+Na)+ 610.2775, found 610.2774.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08088936B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-166da6189c8e4b2782e903d325cb76b5 |
| Source note | uspto-grants-2012_01 |