HCID 66625115, compound → HCID 58286287, compound

Participants

Reaction Steps

A suspension of 2-(2-methoxy-4-nitrophenoxy)ethyl acetate (1.5 g, 5.9 mmol) and Pd/C (Aldrich, 10%, 0.2 g) in ethyl acetate (19 mL) was vigorously shaken in a Parr under atmosphere of H2 (50 psi) for 2 h. The mixture was filtered through a short pad of celite. The filtrate was concentrated to give acetic acid 2-(4-amino-2-methoxy-phenoxy)-ethyl ester as a light brown oil (1.32 g, 91%).

Provenance & Evidence