HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 417523Generated: October 26, 2026
Thionyl Chloride → 4-Bromonaphthalene-1-carbonyl chloride
https://huagongshe.com/reaction/417523
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Bromo-1-naphthoic acid | HCID 282591 | — |
| Product | 4-Bromonaphthalene-1-carbonyl chloride | HCID 14700024 | — |
Reaction Steps
4-Bromonaphthalene-1-carboxylic acid (9.80 g) was suspended in thionyl chloride (80 mL) and stirred at 40° C. for 16 hours and evaporated under vacuum. Solid was dissolved in DCM (20 mL) and evaporated under vacuum, giving 4-bromonaphthalene-1-carbonyl chloride (13.8 g, crude) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08088368B2 |
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| Source dataset | uspto-grants-2012_01 |
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| ORD ID | ord-b78f2ead8cdf4a109a499436f6ca4dc8 |
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| Source note | uspto-grants-2012_01 |
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