Cyclohexylamine → HCID 178516387, compound
Reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([N:10]3[CH:14]([C:15]4[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=4)[C:13](O)=[CH:12][C:11]3=[O:22])=[CH:9][C:4]=2[N:3]=[CH:2]1.[CH:23]1([NH2:29])[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]1>>[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([N:10]3[CH:14]([C:15]4[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=4)[C:13]([NH:29][CH:23]4[CH2:28][CH2:27][CH2:26][CH2:25][CH2:24]4)=[CH:12][C:11]3=[O:22])=[CH:9][C:4]=2[N:3]=[CH:2]1Participants
3
Procedure
The compound was synthesized starting from 1-(1H-benzo[d]imidazol-5-yl)-4-hydroxy-5-phenyl-1H-pyrrol-2(5H)-one (0.120 g, 0.366 mmol) and cyclohexylamine (0.59 ml, 5.13 mmol) according to method 7 described above.
Workup
- customThe compound was synthesized
Sources & evidence
- ORD record
- ord-c860709ec378428190e762b95a1207dc
- Source dataset
- uspto-grants-2013_09
- Patent number
- US08530670B2
Reaction notes
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