HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178482273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 178516575 | HCID 178516575 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Dimethylformamide toluene | HCID 21735183 | — |
| Product | HCID 178482273 | HCID 178482273 | — |
Reaction Steps
The compound was synthesized starting from 1-(1H-benzo[d]imidazol-5-yl)-4-hydroxy-5-(4-morpholinophenyl)-1H-pyrrol-2(5H)-one (0.50 g, 1.32 mmol) and saturated methylamine solution in THF (1 ml) in toluene/DMF (2:1; 5 ml) according to method 8b described above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08530670B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-0e2372ce3a6844acb3519e6603f4abeb |
| Source note | uspto-grants-2013_09 |