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HRID4178

反应详情

EQUATION

反应方程式

HRID 4178 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)SCl
HCID75990

(Chlorothio)formyl chloride

CCl2OS

结构：CC(C)(C)c1cc(C(N)=O)cc(C(C)(C)C)c1O
HCID616502

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)c1cc(-c2nsc(=O)o2)cc(C(C)(C)C)c1O
HCID135778288

未命名化合物

PROCEDURE

实验过程

The procedure of Example 1 is repeated using 3.03 grams of 4-hydroxy-3,5-di-tert-butylbenzamide and 3.18 grams of chlorocarbonylsulfenyl choride. Recrystallization from toluene:heptane (1:1) affords the title compound as a white crystalline solid: mp 155°-157° C. (dec.).

WORKUP

后处理

  1. customRecrystallization from toluene:heptane (1:1)