HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86216469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 23016512 | HCID 23016512 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86216469 | HCID 86216469 | — |
Reaction Steps
100 ml of toluene and 5 g of thionyl chloride were added to the crude product of m-isobutyrylbenzoic acid obtained in the above step (1), and the mixture was reacted under refluxing for 1 hour. After completion of the reaction, excess thionyl chloride was distilled off to obtain a toluene solution of crude m-isobutyrylbenzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093241B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-bcf43c8eaf764a0bb14e252ef375571a |
| Source note | uspto-grants-2012_01 |