HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57713860, compound → HCID 11950887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57713860 | HCID 57713860 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Product | HCID 11950887 | HCID 11950887 | — |
Reaction Steps
The title compound was prepared by cleaving the pivaloyl protecting group of N-[4-chloro-5-(3-diisopropylamino-prop-1-ynyl)-7-(4-methoxy-3,5-dimethyl-pyridin-2-ylmethyl)-7H-pyrrolo[2,3-d]pyrimidin-2-yl]-2,2-dimethyl-propionamide with ZnCl2 according to the General Procedure B. tR: 4.71 min. 1H-NMR (CDCl3) δ 8.24 (s, 1H), 7.05 (s, 1H), 5.30 (s, 2H), 4.96 (s, 1H), 3.76 (s, 3H), 3.68 (s, 2H), 3.27 (7, 2H), 2.27 (s, 2H), 2.20 (s, 2H), 1.15 (d, 12H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093229B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-9ab5a85bfc9a498f91d236b131509776 |
| Source note | uspto-grants-2012_01 |