HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 57431706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Butyl chloroformate | HCID 61140 | — |
| Reactant | 1-Benzylpiperazine | HCID 75994 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57431706 | HCID 57431706 | — |
Reaction Steps
To a solution of 1-benzyl-piperazine (1.97 ml) and NEt3 (1.9 ml) in DCM (100 ml) was added n-butyl chloroformate (1.47 ml). The mixture was stirred at RT for 2 h. Water was added, the org. phase separated, dried (Na2SO4) and evaporated off to give 3.13 g of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093250B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-8295794f02f84bdbad5e76ab0d3ac317 |
| Source note | uspto-grants-2012_01 |