HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propanethiol, sodium salt (1:1) → HCID 57863107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propanethiol, sodium salt (1:1) | HCID 4681725 | — |
| Reactant | 3,5-Dibromoanisole | HCID 11021812 | — |
| Product | HCID 57863107 | HCID 57863107 | 39% |
Reaction Steps
A similar procedure as described in Example 47, step 2 was used, starting from 3,5-dibromoanisole (5.3 g, 19.93 mmol) and sodium 1-propanethiolate (2.47 g, 23.92 mmol) to afford 1-bromo-3-methoxy-5-propylsulfanyl-benzene (2.01 g, 39%) as a light yellow oil: EI(+)-HRMS m/e calcd for C10H13BrOS (M)+ 259.9870, found 259.9870.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093253B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-4ee702b9fbe64bbfa5f5fb508494a4b5 |
| Source note | uspto-grants-2012_01 |