Boron tribromide → HCID 57863101, compound

Participants

Reaction Steps

A similar procedure as described in Example 47, step 4 was used, starting from 1-bromo-3-methoxy-5-(propane-1-sulfonyl)-benzene (1.55 g, 5.29 mmol) and boron tribromide (10.57 mL, 10.57 mmol, 1.0M in dichloromethane) to afford 3-bromo-5-(propane-1-sulfonyl)-phenol (1.15 g, 78%) as a white solid: ES(+)-HRMS m/e calcd for C9H11BrO3S (M+Na)+ 300.9504, found 300.9503.

Provenance & Evidence