化工社化工社 化学情報印刷レポート · 研究参考用
Nitrate → 3-Iodo-5-(5-methyl-pyridin-2-yl)-benzoic acid methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitrate | HCID 943 | — |
| 反応物 | Diiodomethane | HCID 6346 | — |
| 反応物 | Methyl 3-amino-5-(5-methylpyridin-2-yl)benzoate | HCID 57851018 | — |
| 生成物 | 3-Iodo-5-(5-methyl-pyridin-2-yl)-benzoic acid methyl ester | HCID 59432579 | — |
反応手順
3-Amino-5-(5-methyl-pyridin-2-yl)-benzoic acid methyl ester was treated with methylene iodide and isoamy nitrate using the procedure of step 3 of preparation 4, to afford 3-iodo-5-(5-methyl-pyridin-2-yl)-benzoic acid methyl ester, MS (M+H)=353.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08093275B2 |
| 出典データセット | uspto-grants-2012_01 |
| ORD ID | ord-8118940bf4974d71b999d7135cc11f2c |
| 出典メモ | uspto-grants-2012_01 |