HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 59515704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 59515798 | HCID 59515798 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 59515704 | HCID 59515704 | — |
Reaction Steps
A mixture of (R)-2-(6-methoxy-5-nitro-1-oxoisoquinolin-2(1H)-yl)propanamide (200 mg, 0.0007 mol), methanol (20 mL, 0.5 mol) and palladium, 10% weight on charcoal (21 mg, 0.00017 mol) was stirred under hydrogen (1 atm) for 3 h. The reaction mixture was filtered over celite and the solvent was removed to afford the product as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08093265B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-a0aa7fb93a1c4fa08ccbb519eee8823a |
| Source note | uspto-grants-2012_01 |