Phenylhydrazine hydrochloride → 2,6-Dibromo-4-methylbenzaldehyde phenylhydrazone

HRID 418789Notes

Reaction equation

HRID 418789 reaction equation
F[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][N:9]=[CH:10][C:11]1[C:16]([Br:17])=[CH:15][C:14]([CH3:18])=[CH:13][C:12]=1[Br:19].BrC1C=C(C)C=C(Br)C=1C=O.Cl.C1(NN)C=CC=CC=1>>[C:3]1([NH:8][N:9]=[CH:10][C:11]2[C:12]([Br:19])=[CH:13][C:14]([CH3:18])=[CH:15][C:16]=2[Br:17])[CH:4]=[CH:5][CH:6]=[CH:7][CH:2]=1

Participants

4

Reactant 3

HCID 60962Phenylhydrazine hydrochlorideHCID 129827482,6-Dibromo-4-methylbenzaldehydeHCID 666488172,6-Dibromo-4-methylbenzaldehyde (2-fluorophenyl)hydrazone

Product 1

HCID 666483122,6-Dibromo-4-methylbenzaldehyde phenylhydrazone

Procedure

Similarly prepared to Intermediate 25 from 2,6-dibromo-4-methylbenzaldehyde and phenylhydrazine hydrochloride.

Sources & evidence

ORD record
ord-40b796f93a7b459ea1bdae3e83119b65
Source dataset
uspto-grants-2012_01
Patent number
US08093281B2

Reaction notes

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