Cyclohexene oxide → HCID 66652046, compound

HRID 418931Notes

Reaction equation

HRID 418931 reaction equation
[CH:1]12[O:7][CH:2]1[CH2:3][CH2:4][CH2:5][CH2:6]2.Br[C:9]1[CH:14]=[C:13]([O:15][CH3:16])[CH:12]=[C:11]([O:17][CH3:18])[CH:10]=1>>[CH3:16][O:15][C:13]1[CH:14]=[C:9]([CH:2]2[CH2:3][CH2:4][CH2:5][CH2:6][CH:1]2[OH:7])[CH:10]=[C:11]([O:17][CH3:18])[CH:12]=1

Participants

3

Reactant 2

HCID 9246Cyclohexene oxideHCID 6391871-Bromo-3,5-dimethoxybenzene

Product 1

HCID 66652046HCID 66652046, compound

Procedure

Preparation 106 is prepared from cyclohexene oxide and 1-bromo-3,5-dimethoxybenzene in a manner similar to preparation 10. 1H NMR (CDCl3): 6.41 (s, 2H), 6.35(s, 1H), 3.79 (s, 6H), 3.65 (m, 1H), 2.37 (m, 1H), 2.1 (m, 1H), 1.85 (m, 2H), 1.75 (m, 1H)1.6-1.2 (m, 4H).

Workup

  1. customPreparation 106

Sources & evidence

ORD record
ord-1707e041a1a34dba887a3e39678907b6
Source dataset
uspto-grants-2012_01
Patent number
US08093302B2

Reaction notes

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