HCID 66651877, compound → HCID 66652075, compound

Participants

Reaction Steps

Combine 7-Isopropenyl-6-methoxy-10-(4-methoxy-phenyl)-1,2,3,4,4a,9,10,10a-octahydro-phenanthrene (0.14 g, 0.39 mmol) and 10% Pd/C (0.13 g) and reduce at 50 psi of H2O.N. Filter catalyst and remove solvent in vacuo to yield the titled compound (0.13 g, 93%). 1H NMR (CDCl3): 7.28 (d, J=8.4 Hz, 2H), 7.02 (s, 1H), 6.92 (d, J=8.8 HZ, 2H), 6.89 (s, 1H), 3.87 (s, 3H), 3.85 (s, 3H), 3.25 (m, 4H), 2.85 (m, 1H), 2.5 (m, 1H), 2.06 (m, 1H), 1.8-1.1 (m, 13H).

Provenance & Evidence