HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 419762Generated: October 31, 2026
Pyridine → N-(2-bromophenyl)-4-methoxybenzamide
https://huagongshe.com/reaction/419762
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | 2-Bromoaniline | HCID 11992 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-(2-bromophenyl)-4-methoxybenzamide | HCID 5176555 | — |
Reaction Steps
To a suspension of 2-bromoaniline (7.3 mL) and pyridine (13.5 mL) in toluene (110 mL) was added 4-methoxybenzoyl chloride (11 mL) and the mixture was heated at 40° C. for 2.5 hours. The solid was filtered, washed with diethyl ether and water and dried to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08093396B2 |
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| Source dataset | uspto-grants-2012_01 |
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| ORD ID | ord-b0d171b60c824288b7d2ae32b435a8a1 |
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| Source note | uspto-grants-2012_01 |
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