Hydrochloric Acid → HCID 66651598, compound

Participants

Reaction Steps

To a solution of EXAMPLE 1C (5 g) in N,N-dimethylformamide (1.6 mL) was added copper(I) cyanide (2.1 g) and the mixture heated at reflux for 6 hours. The mixture was cooled, poured into 1N hydrochloric acid and extracted with ethyl acetate. The solid that precipitated out of the organic layer was filtered, washed with water and dried to afford the title compound.

Provenance & Evidence