HRID419808

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2757709

4-chloro-3-methylpyridine

C6H6ClN

结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@H](OC(C)=O)CS[C@H]1Oc1cncc(Br)c1

HCID44195502

未命名化合物

PRODUCTS

生成物

结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@H](OC(C)=O)CS[C@H]1Oc1cncc(-c2ccncc2C)c1

HCID66650769

未命名化合物

PROCEDURE

实验过程

By carrying out the operation analogously to example 49, starting from 5-bromo-3-pyridinyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside, obtained according to preparation IX, and 4-chloro-3-methylpyridine, the desired product is obtained in the form of beige crystals (yield=15%).

WORKUP

后处理

customobtained