HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dibromo-5-nitropyridine → 3-Bromo-2-(3-methoxyphenyl)-5-nitropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dibromo-5-nitropyridine | HCID 1201425 | — |
| Reactant | (3-Methoxyphenyl)boronic acid | HCID 2734370 | — |
| Product | 3-Bromo-2-(3-methoxyphenyl)-5-nitropyridine | HCID 67394339 | 40% |
Reaction Steps
Obtained (1.15 g, yield 40%) following the procedure described in Intermediate 27, starting with 2,3-dibromo-5-nitropyridine (9.33 mmol, 2.63 g), 3-methoxyphenylboronic acid (9.33 mmol, 1.42 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536165B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-25052060f24c4cf4829bdca9ffbbbed8 |
| Source note | uspto-grants-2013_09 |