7-Bromooct-1-ene → n-Methyloct-5-en-1-amine tosylate salt

HRID 420029Notes

Reaction equation

HRID 420029 reaction equation
Br[CH:2]([CH3:9])[CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8].[S:10]([C:14]1[CH:20]=[CH:19][C:17]([CH3:18])=[CH:16][CH:15]=1)([OH:13])(=[O:12])=[O:11].[CH3:21][NH:22]CCCCC=C>>[S:10]([C:14]1[CH:20]=[CH:19][C:17]([CH3:18])=[CH:16][CH:15]=1)([OH:13])(=[O:12])=[O:11].[CH3:21][NH:22][CH2:9][CH2:2][CH2:3][CH2:4][CH:5]=[CH:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 221384327-Bromooct-1-eneHCID 46737741N-methylhex-5-en-1-amine 4-methylbenzenesulfonate

Product 1

HCID 131729113n-Methyloct-5-en-1-amine tosylate salt

Procedure

Compound 32c was synthesized from 7-bromo-octene as a white powder in quantitative yield, following the procedure as described for compound 32a.

Sources & evidence

ORD record
ord-5b5e84dcfee14f1fa3e26f62d06056b2
Source dataset
uspto-grants-2012_01
Patent number
US08093379B2

Reaction notes

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