HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Carbamoylphenyl)boronic acid → 3-(3-Methyl-5-nitropyridin-2-yl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Carbamoylphenyl)boronic acid | HCID 2737814 | — |
| Reactant | 2-Bromo-3-methyl-5-nitropyridine | HCID 5200466 | — |
| Product | 3-(3-Methyl-5-nitropyridin-2-yl)benzamide | HCID 67394166 | 95% |
Reaction Steps
Obtained (0.225 g, yield 95%) following the procedure described in Intermediate 27, starting with 2-bromo-3-methyl-5-nitropyridine (0.92 mmol, 0.200 g), 3-carbamoylphenyl boronic acid (0.92 mmol, 0.152 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536165B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-7f080017fac3419a8fc81fdf3499b97c |
| Source note | uspto-grants-2013_09 |