3-Pyridinylboronic acid → HCID 57586462, compound

Participants

Reaction Steps

A similar procedure as described in Example 1, step 2 was used, starting from 4-{3-[6-(3,5-dibromo-phenoxy)-hexyl]-2-(2-ethoxycarbonyl-ethyl)-phenoxy}-butyric acid ethyl ester (250 mg, 0.39 mmol) and pyridin-3-ylboronic acid (201 mg, 1.55 mmol) to give 4-{3-[6-(3,5-di-pyridin-3-yl-phenoxy)-hexyl]-2-(2-ethoxycarbonyl-ethyl)-phenoxy}-butyric acid ethyl ester (155 mg, 62%) as a colorless oil: ES(+)-HRMS m/e calculated for C39H46N2O6 (M+H)+ 639.3429, found 639.3416.

Provenance & Evidence