Octylamine → HCID 86626136, compound

HRID 420429Notes

Reaction equation

HRID 420429 reaction equation
[CH2:1]([O:13][S:14]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)(=[O:16])=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:23]([NH2:31])[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]>>[CH2:23]([NH2:31])[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30].[CH2:1]([O:13][S:14]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)(=[O:16])=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 8143OctylamineHCID 15900Dodecyl benzenesulfonate

Product 1

HCID 86626136HCID 86626136, compound

Procedure

1200 g of branched dodecylbenzenesulfonate was heated (50 to 60° C.) while being stirred. Octylamine was added dropwise while keeping the temperature constant (50 to 60° C.) until the pH of the system increased to approximately 6 to obtain a branched dodecylbenzenesulfonate octylamine salt.

Workup

  1. customthe temperature constant (50 to 60° C.)
  2. temperatureincreased to approximately 6

Sources & evidence

ORD record
ord-b70c5ef96b224ab9945b799894afcc69
Source dataset
uspto-grants-2012_01
Patent number
US08097563B2

Reaction notes

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