HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichlorobenzoic acid → 2-(6-Bromo-5-methylpyridin-3-ylamino)-5-chlorobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichlorobenzoic acid | HCID 5784 | — |
| Reactant | 5-Amino-2-bromo-3-methylpyridine | HCID 12362446 | — |
| Product | 2-(6-Bromo-5-methylpyridin-3-ylamino)-5-chlorobenzoic acid | HCID 86657260 | 24% |
Reaction Steps
Obtained (0.51 g, yield 24%) following the procedure described in Intermediate 13 starting with 6-bromo-5-methylpyridin-3-amine (5.35 mmol, 1.0 g) and 2,5-dichlorobenzoic acid (10.68 mmol, 2.04 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536165B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-c1621bb7fc9d48d491d4c64871edc448 |
| Source note | uspto-grants-2013_09 |