HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-methylbenzoic Acid → 2-(6-Bromo-5-methylpyridin-3-ylamino)-5-methylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-methylbenzoic Acid | HCID 240430 | — |
| Reactant | 5-Amino-2-bromo-3-methylpyridine | HCID 12362446 | — |
| Product | 2-(6-Bromo-5-methylpyridin-3-ylamino)-5-methylbenzoic acid | HCID 86657261 | 20% |
Reaction Steps
Obtained (0.51 g, yield 20%) following the procedure described in Intermediate 13 starting with 6-bromo-5-methylpyridin-3-amine (7.70 mmol, 1.44 g) and 2-chloro-5-methylbenzoic acid (15.36 mmol, 2.62 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536165B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-c1782b7f95e34dc7bf20523e46da8acb |
| Source note | uspto-grants-2013_09 |