HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → tert-Butyl 2-(5-chloro-6-phenylpyridin-3-ylamino)-5-methylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | Tert-butyl 2-(2-bromo-5-chloropyridin-3-ylamino)-5-methylbenzoate | HCID 58415802 | — |
| Product | tert-Butyl 2-(5-chloro-6-phenylpyridin-3-ylamino)-5-methylbenzoate | HCID 86657263 | — |
Reaction Steps
Obtained (0.005 g, 3% of yield) following the procedure described in Example 8 (step A) starting with 0.230 g (0.58 mmol) of Intermediate 20A and 0.106 g (0.87 mmol) of phenylboronic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536165B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-51e0fb53203e4f64a685adf403811cac |
| Source note | uspto-grants-2013_09 |