Ethylenediamine → HCID 66658117, compound

HRID 420856Notes

Reaction equation

HRID 420856 reaction equation
[C:1]([C:4]1[CH:18]=[CH:17][C:7]([O:8][CH2:9][C:10]([N:12]([CH2:15][CH3:16])[CH2:13][CH3:14])=[O:11])=[CH:6][CH:5]=1)(=O)[CH3:2].[CH2:19]([NH2:22])[CH2:20][NH2:21]>C(O)(=O)C>[NH2:21][CH2:20][CH2:19][NH:22][CH:1]([C:4]1[CH:18]=[CH:17][C:7]([O:8][CH2:9][C:10]([N:12]([CH2:15][CH3:16])[CH2:13][CH3:14])=[O:11])=[CH:6][CH:5]=1)[CH3:2]

Participants

4

Reactant 2

HCID 3301EthylenediamineHCID 24924572-(4-Acetylphenoxy)-N,N-diethylacetamide

Product 1

HCID 66658117HCID 66658117, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

By using 2-(4-acetylphenoxy)-N,N-diethylacetamide (250 mg), ethylenediamine (400 μl) and acetic acid (700 μl) as starting materials, the title compound (52.9 mg) was obtained in the same manner as that of Reference Example 64, (1).

Sources & evidence

ORD record
ord-aa4ec809cd974f9d95732614f19dbc36
Source dataset
uspto-grants-2012_01
Patent number
US08097708B2

Reaction notes

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